Information card for entry 7124303

Structure parameters

• Formula: C28 H28 N2 Si
• Calculated formula: C28 H28 N2 Si
• Title of publication: Lewis Acid-Catalyzed Synthesis of Silafluorene Derivatives from Biphenyls and Dihydrosilanes via Double Sila-Friedel-Crafts Reaction
• Authors of publication: Dong, Yafang; Takata, Yuta; Yoshigoe, Yusuke; Sekine, Kohei; Kuninobu, Yoichiro
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 9.4768 ± 0.0004 Å
• b: 10.9099 ± 0.0004 Å
• c: 13.1313 ± 0.0005 Å
• α: 113.798 ± 0.003°
• β: 91.992 ± 0.004°
• γ: 112.004 ± 0.004°
• Cell volume: 1123.73 ± 0.09 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.11
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No