Information card for entry 7124373

Structure parameters

• Formula: C27 H43 F N O P Si
• Calculated formula: C27 H43 F N O P Si
• Title of publication: Palladium-Catalyzed Regioselective C−H Alkynylation of Indoles with Haloalkynes: Access to Functionalized 7-Alkynylindoles
• Authors of publication: Wu, Wanqing; Fang, Songjia; Jiang, Guangbin; Li, Meng; Liu, Zhenying; Jiang, Huanfeng
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 11.936 ± 0.003 Å
• b: 10.888 ± 0.002 Å
• c: 22.186 ± 0.005 Å
• α: 90°
• β: 95.814 ± 0.006°
• γ: 90°
• Cell volume: 2868.4 ± 1.1 ų
• Cell temperature: 220 K
• Ambient diffraction temperature: 220 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1315
• Residual factor for significantly intense reflections: 0.0633
• Weighted residual factors for significantly intense reflections: 0.1297
• Weighted residual factors for all reflections included in the refinement: 0.1558
• Goodness-of-fit parameter for all reflections included in the refinement: 0.903
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No