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Information card for entry 7124563
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Coordinates | 7124563.cif |
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Original paper (by DOI) | HTML |
Common name | Os(ONO)2 . 2 CHCl3 |
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Chemical name | Bis[bis(3,5-di-tert-butyl-2-oxyphenyl)amido]osmium dichloroform solvate |
Formula | C58 H82 Cl6 N2 O4 Os |
Calculated formula | C56.5 H80.5 Cl1.5 N2 O4 Os |
Title of publication | Octahedral to trigonal prismatic distortion driven by subjacent orbital π antibonding interactions and modulated by ligand redox noninnocence. |
Authors of publication | Cipressi, Jacqueline; Brown, Seth N. |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2014 |
Journal volume | 50 |
Journal issue | 59 |
Pages of publication | 7956 - 7959 |
a | 59.4673 ± 0.0019 Å |
b | 21.5249 ± 0.0006 Å |
c | 19.0986 ± 0.0005 Å |
α | 90° |
β | 95.211 ± 0.003° |
γ | 90° |
Cell volume | 24345.7 ± 1.2 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0689 |
Residual factor for significantly intense reflections | 0.0595 |
Weighted residual factors for significantly intense reflections | 0.1458 |
Weighted residual factors for all reflections included in the refinement | 0.1506 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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