Information card for entry 7124609

Structure parameters

• Formula: C88 H38 Al B2 Br F40 N4
• Calculated formula: C88 H38 Al B2 Br F40 N4
• Title of publication: Cationic aluminum hydride complexes: reactions of carbene-alane adducts with trityl-borate.
• Authors of publication: Cao, Levy L.; Daley, Erika; Johnstone, Timothy C.; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 30
• Pages of publication: 5305 - 5307
• a: 12.4696 ± 0.001 Å
• b: 13.5438 ± 0.001 Å
• c: 23.9484 ± 0.0019 Å
• α: 89.208 ± 0.004°
• β: 88.213 ± 0.004°
• γ: 79.504 ± 0.004°
• Cell volume: 3974.8 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.12
• Residual factor for significantly intense reflections: 0.074
• Weighted residual factors for significantly intense reflections: 0.2112
• Weighted residual factors for all reflections included in the refinement: 0.2421
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No