Information card for entry 7124620

Structure parameters

• Common name: (BDI)Nb(NtBu)Ph
• Formula: C39 H54 N3 Nb
• Calculated formula: C39 H54 N3 Nb
• Title of publication: Photo-activation of d(0) niobium imido azides: en route to nitrido complexes.
• Authors of publication: Camp, Clément; Grant, Lauren N.; Bergman, Robert G.; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 32
• Pages of publication: 5538 - 5541
• a: 9.6363 ± 0.0004 Å
• b: 10.354 ± 0.0004 Å
• c: 10.4978 ± 0.0004 Å
• α: 107.019 ± 0.001°
• β: 113.605 ± 0.001°
• γ: 91.585 ± 0.001°
• Cell volume: 905.11 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.0773
• Weighted residual factors for all reflections included in the refinement: 0.0786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: mokα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No