Information card for entry 7124666

Structure parameters

• Formula: C31 H35 N O2 Si
• Calculated formula: C31 H35 N O2 Si
• Title of publication: Efficient access to alkynylated quinalizinones via the gold(i)-catalyzed aminoalkynylation of alkynes.
• Authors of publication: Shinde, Popat S.; Shaikh, Aslam C.; Patil, Nitin T.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 52
• Pages of publication: 8152 - 8155
• a: 10.5604 ± 0.0007 Å
• b: 12.5871 ± 0.001 Å
• c: 20.6289 ± 0.0015 Å
• α: 90°
• β: 103.411 ± 0.003°
• γ: 90°
• Cell volume: 2667.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0425
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0898
• Weighted residual factors for all reflections included in the refinement: 0.093
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No