Information card for entry 7124695

Structure parameters

• Formula: C21 H30 Li N3
• Calculated formula: C21 H30 Li N3
• Title of publication: The importance of the Lewis base in lithium mediated metallation and bond cleavage reaction of allyl amines and allyl phosphines.
• Authors of publication: Blair, V. L.; Stevens, M. A.; Thompson, C. D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 52
• Pages of publication: 8111 - 8114
• a: 10.1048 ± 0.0008 Å
• b: 12.9834 ± 0.0008 Å
• c: 15.341 ± 0.001 Å
• α: 90°
• β: 102.567 ± 0.004°
• γ: 90°
• Cell volume: 1964.4 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0502
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1103
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No