Information card for entry 7124697

Structure parameters

• Formula: C24 H37 Li N4
• Calculated formula: C24 H37 Li N4
• Title of publication: The importance of the Lewis base in lithium mediated metallation and bond cleavage reaction of allyl amines and allyl phosphines.
• Authors of publication: Blair, V. L.; Stevens, M. A.; Thompson, C. D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 52
• Pages of publication: 8111 - 8114
• a: 10.1275 ± 0.0004 Å
• b: 8.6095 ± 0.0003 Å
• c: 27.5008 ± 0.0012 Å
• α: 90°
• β: 91.558 ± 0.003°
• γ: 90°
• Cell volume: 2396.98 ± 0.16 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0898
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.0979
• Weighted residual factors for all reflections included in the refinement: 0.1154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.005
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No