Information card for entry 7124724

Structure parameters

• Formula: C84 H93.9 Br2 F24 N19.05 O0.47 P2 Sb4
• Calculated formula: C84 H93.896 Br2 F24 N19.052 O0.474 P2 Sb4
• Title of publication: Bis(carbodicarbene)phosphenium trication: the case against hypervalency.
• Authors of publication: Đorđević, Nemanja; Ganguly, Rakesh; Petković, Milena; Vidović, Dragoslav
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 63
• Pages of publication: 9789 - 9792
• a: 12.1048 ± 0.0003 Å
• b: 13.7318 ± 0.0004 Å
• c: 16.1379 ± 0.0005 Å
• α: 108.884 ± 0.0016°
• β: 98.2298 ± 0.0014°
• γ: 102.753 ± 0.0014°
• Cell volume: 2407.61 ± 0.12 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.117
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.0988
• Weighted residual factors for all reflections included in the refinement: 0.1178
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No