Crystallography Open Database

Information card for entry 7124876

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Coordinates	7124876.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C115 N10 O77 Si2 Sn6 W18
Calculated formula	C115 N10 O77 Si2 Sn6 W18
Title of publication	Hexanuclear tin(ii) and mixed valence tin(ii,iv) oxide clusters within polyoxometalates.
Authors of publication	Suzuki, Kosuke; Hanaya, Takumi; Sato, Rinta; Minato, Takuo; Yamaguchi, Kazuya; Mizuno, Noritaka
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2016
Journal volume	52
Journal issue	70
Pages of publication	10688 - 10691
a	17.6999 ± 0.0002 Å
b	18.7362 ± 0.0002 Å
c	29.8744 ± 0.0004 Å
α	82.659 ± 0.001°
β	88.278 ± 0.001°
γ	74.291 ± 0.001°
Cell volume	9458.9 ± 0.2 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1126
Residual factor for significantly intense reflections	0.0767
Weighted residual factors for significantly intense reflections	0.1869
Weighted residual factors for all reflections included in the refinement	0.2039
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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