Information card for entry 7124908

Structure parameters

• Formula: C33 H53 B Br N3 O Si Zn
• Calculated formula: C33 H53 B Br N3 O Si Zn
• Title of publication: Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
• Authors of publication: Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 69
• Pages of publication: 10490 - 10492
• a: 15.203 ± 0.003 Å
• b: 11.974 ± 0.002 Å
• c: 19.965 ± 0.004 Å
• α: 90°
• β: 100.3 ± 0.03°
• γ: 90°
• Cell volume: 3575.9 ± 1.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for significantly intense reflections: 0.0676
• Weighted residual factors for all reflections included in the refinement: 0.0739
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No