Information card for entry 7124910

Structure parameters

• Formula: C42 H48.98 Br0.02 N Si Zn
• Calculated formula: C42 H48.9793 Br0.02065 N Si Zn
• Title of publication: Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
• Authors of publication: Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 69
• Pages of publication: 10490 - 10492
• a: 14.0869 ± 0.0004 Å
• b: 15.8901 ± 0.0005 Å
• c: 17.1769 ± 0.0005 Å
• α: 72.101 ± 0.001°
• β: 81.448 ± 0.001°
• γ: 81.036 ± 0.001°
• Cell volume: 3593.29 ± 0.19 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.046
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.11
• Weighted residual factors for all reflections included in the refinement: 0.114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No