Information card for entry 7124960

Structure parameters

• Formula: C19 H20 N2 O2 S
• Calculated formula: C19 H20 N2 O2 S
• Title of publication: A visible-light photocatalytic N-radical cascade of hydrazones for the synthesis of dihydropyrazole-fused benzosultams.
• Authors of publication: Zhao, Quan-Qing; Hu, Xiao-Qiang; Yang, Meng-Nan; Chen, Jia-Rong; Xiao, Wen-Jing
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 86
• Pages of publication: 12749 - 12752
• a: 9.31 ± 0.0009 Å
• b: 13.2449 ± 0.0013 Å
• c: 14.8906 ± 0.0015 Å
• α: 69.506 ± 0.001°
• β: 77.927 ± 0.001°
• γ: 89.163 ± 0.001°
• Cell volume: 1678.5 ± 0.3 ų
• Cell temperature: 100.15 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.112
• Weighted residual factors for all reflections included in the refinement: 0.1181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No