Information card for entry 7125008
| Formula |
C18 H22 Br P Te |
| Calculated formula |
C18 H22 Br P Te |
| Title of publication |
Increasing the Brønsted acidity of Ph2PO2H by the Lewis acid B(C6F5)3. Formation of an eight-membered boraphosphinate ring [Ph2POB(C6F5)2O]2. |
| Authors of publication |
Kather, Ralf; Rychagova, Elena; Sanz Camacho, Paula; Ashbrook, Sharon E.; Woollins, J. Derek; Robben, Lars; Lork, Enno; Ketkov, Sergey; Beckmann, Jens |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2016 |
| Journal volume |
52 |
| Journal issue |
73 |
| Pages of publication |
10992 - 10995 |
| a |
7.786 ± 0.0008 Å |
| b |
13.9267 ± 0.0014 Å |
| c |
16.4054 ± 0.0018 Å |
| α |
90° |
| β |
97.078 ± 0.007° |
| γ |
90° |
| Cell volume |
1765.3 ± 0.3 Å3 |
| Cell temperature |
125 K |
| Ambient diffraction temperature |
125 K |
| Number of distinct elements |
5 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/n 1 |
| Hall space group symbol |
-P 2yn |
| Residual factor for significantly intense reflections |
0.023 |
| Weighted residual factors for all reflections included in the refinement |
0.0536 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.037 |
| Diffraction radiation wavelength |
0.71075 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7125008.html
