Information card for entry 7125041
| Formula |
C28 H21 Br O3 |
| Calculated formula |
C28 H21 Br O3 |
| Title of publication |
Dual rhodium/copper catalysis: synthesis of benzo[b]fluorenes and 2-naphthalenylmethanones via de-diazotized cycloadditions. |
| Authors of publication |
Wu, Ya-Nan; Xu, Ting; Fu, Rong; Wang, Nan-Nan; Hao, Wen-Juan; Wang, Shu-Liang; Li, Guigen; Tu, Shu-Jiang; Jiang, Bo |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2016 |
| Journal volume |
52 |
| Journal issue |
80 |
| Pages of publication |
11943 - 11946 |
| a |
7.336 ± 0.0007 Å |
| b |
11.8041 ± 0.0009 Å |
| c |
13.6969 ± 0.0011 Å |
| α |
104.265 ± 0.002° |
| β |
98.881 ± 0.001° |
| γ |
96.225 ± 0.001° |
| Cell volume |
1122.36 ± 0.16 Å3 |
| Cell temperature |
298 ± 2 K |
| Ambient diffraction temperature |
298 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0982 |
| Residual factor for significantly intense reflections |
0.0445 |
| Weighted residual factors for significantly intense reflections |
0.0834 |
| Weighted residual factors for all reflections included in the refinement |
0.0898 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.054 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7125041.html
