Information card for entry 7125126

Structure parameters

• Formula: C59 H69 N Sn2
• Calculated formula: C59 H69 N Sn2
• Title of publication: Catalytic dehydrocoupling of amines and boranes by an incipient tin(ii) hydride.
• Authors of publication: Erickson, Jeremy D.; Lai, Ting Yi; Liptrot, David J.; Olmstead, Marilyn M.; Power, Philip P.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 94
• Pages of publication: 13656 - 13659
• a: 25.5341 ± 0.0012 Å
• b: 22.081 ± 0.0011 Å
• c: 21.1566 ± 0.0016 Å
• α: 90°
• β: 122.336 ± 0.0011°
• γ: 90°
• Cell volume: 10078.7 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0525
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.109
• Weighted residual factors for all reflections included in the refinement: 0.1123
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No