Information card for entry 7125128

Structure parameters

• Formula: C32 H30 Cl2 I2 N P Pd
• Calculated formula: C32 H30 Cl2 I2 N P Pd
• Title of publication: Isolation and properties of a palladium PBP pincer complex featuring an ambiphilic boryl site.
• Authors of publication: Schuhknecht, Danny; Ritter, Florian; Tauchert, Michael E.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 79
• Pages of publication: 11823 - 11826
• a: 9.0882 ± 0.0006 Å
• b: 10.5044 ± 0.0007 Å
• c: 16.7224 ± 0.0012 Å
• α: 82.47 ± 0.001°
• β: 80.174 ± 0.001°
• γ: 86.84 ± 0.001°
• Cell volume: 1558.56 ± 0.18 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0374
• Residual factor for significantly intense reflections: 0.0324
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No