Information card for entry 7125132

Structure parameters

• Chemical name: RK-53
• Formula: C24 H42 B O6 P Si2 W
• Calculated formula: C24 H42 B O6 P Si2 W
• Title of publication: Synthesis of a monomolecular anionic FLP complex.
• Authors of publication: Kyri, A. W.; Kunzmann, R.; Schnakenburg, G.; Qu, Z.-W.; Grimme, S.; Streubel, R.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 91
• Pages of publication: 13361 - 13364
• a: 19.042 ± 0.006 Å
• b: 9.093 ± 0.003 Å
• c: 35.451 ± 0.011 Å
• α: 90°
• β: 94.657 ± 0.005°
• γ: 90°
• Cell volume: 6118 ± 3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0569
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.1006
• Weighted residual factors for all reflections included in the refinement: 0.1087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No