Information card for entry 7125184

Structure parameters

• Formula: C59 H88 N5 O Sm
• Calculated formula: C59 H88 N5 O Sm
• Title of publication: Sterically induced reductive linkage of iron polypnictides with bulky lanthanide complexes by ring-opening of THF.
• Authors of publication: Schoo, Christoph; Bestgen, Sebastian; Schmidt, Monika; Konchenko, Sergey N.; Scheer, Manfred; Roesky, Peter W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 90
• Pages of publication: 13217 - 13220
• a: 12.769 ± 0.002 Å
• b: 13.1625 ± 0.0014 Å
• c: 20.932 ± 0.003 Å
• α: 76.406 ± 0.01°
• β: 80.735 ± 0.012°
• γ: 63.678 ± 0.009°
• Cell volume: 3058.5 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0652
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0689
• Weighted residual factors for all reflections included in the refinement: 0.0734
• Goodness-of-fit parameter for all reflections included in the refinement: 0.832
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No