Information card for entry 7125200

Structure parameters

• Formula: C14 H34 Cl2 F3 Li O7 S Si4
• Calculated formula: C14 H34 Cl2 F3 Li O7 S Si4
• Title of publication: Synthesis and coordination ability of a partially silicon based crown ether.
• Authors of publication: Reuter, Kirsten; Thiele, Günther; Hafner, Thomas; Uhlig, Frank; von Hänisch, Carsten
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 90
• Pages of publication: 13265 - 13268
• a: 14.6745 ± 0.0007 Å
• b: 24.0048 ± 0.0011 Å
• c: 32.5952 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11481.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0763
• Residual factor for significantly intense reflections: 0.0534
• Weighted residual factors for significantly intense reflections: 0.1174
• Weighted residual factors for all reflections included in the refinement: 0.1273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No