Information card for entry 7125288
| Formula |
C23 H27 N3 O2 |
| Calculated formula |
C23 H27 N3 O2 |
| Title of publication |
Selective Tsuji-Trost type C-allylation of hydrazones: a straightforward entry into 4,5-dihydropyrazoles. |
| Authors of publication |
El Mamouni, El Hachemia; Cattoen, Martin; Cordier, Marie; Cossy, Janine; Arseniyadis, Stellios; Ilitki, Hocine; El Kaïm, Laurent |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2016 |
| Journal volume |
52 |
| Journal issue |
100 |
| Pages of publication |
14490 - 14493 |
| a |
8.2014 ± 0.0004 Å |
| b |
10.9469 ± 0.0006 Å |
| c |
12.241 ± 0.0004 Å |
| α |
99.951 ± 0.003° |
| β |
94.49 ± 0.003° |
| γ |
103.679 ± 0.002° |
| Cell volume |
1043.58 ± 0.09 Å3 |
| Cell temperature |
150 ± 0.1 K |
| Ambient diffraction temperature |
150 ± 0.1 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0948 |
| Residual factor for significantly intense reflections |
0.0597 |
| Weighted residual factors for significantly intense reflections |
0.1259 |
| Weighted residual factors for all reflections included in the refinement |
0.1458 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.097 |
| Diffraction radiation wavelength |
0.71069 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7125288.html
