Information card for entry 7125674

Structure parameters

• Formula: C56 H41 B F20 N O P
• Calculated formula: C56 H41 B F20 N O P
• Title of publication: Isolable cyclic (alkyl)(amino)carbene-phosphonyl radical adducts.
• Authors of publication: Livshits-Kritsman, Yulia; Tumanskii, Boris; Ménard, Gabriel; Dobrovetsky, Roman
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 9
• Pages of publication: 1341 - 1344
• a: 35.439 ± 0.004 Å
• b: 35.468 ± 0.004 Å
• c: 7.9392 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9979.2 ± 1.9 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 7
• Space group number: 32
• Hermann-Mauguin space group symbol: P b a 2
• Hall space group symbol: P 2 -2ab
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.0911
• Weighted residual factors for all reflections included in the refinement: 0.0982
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No