Information card for entry 7125676

Structure parameters

• Formula: C32 H41 N O P
• Calculated formula: C32 H41 N O P
• Title of publication: Isolable cyclic (alkyl)(amino)carbene-phosphonyl radical adducts.
• Authors of publication: Livshits-Kritsman, Yulia; Tumanskii, Boris; Ménard, Gabriel; Dobrovetsky, Roman
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 9
• Pages of publication: 1341 - 1344
• a: 10.5072 ± 0.0003 Å
• b: 14.0611 ± 0.0003 Å
• c: 18.7738 ± 0.0005 Å
• α: 90°
• β: 103.585 ± 0.001°
• γ: 90°
• Cell volume: 2696.09 ± 0.12 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.1056
• Weighted residual factors for all reflections included in the refinement: 0.1129
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No