Information card for entry 7125686

Structure parameters

• Formula: C152 H254 As16 N16 Na6 O72 Sn14
• Calculated formula: C152 H190 As16 N16 Na6 O60 Sn14
• Title of publication: A core-shell type alkyl-Sn-oxo cluster of {Sn₁₄As₁₆} bridged by 4-aminophenylarsonate ligands and incorporated with a {Na₆} cluster.
• Authors of publication: Zhu, Yu; Zhang, Jian; Zhang, Lei
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 9
• Pages of publication: 1433 - 1435
• a: 28.003 ± 0.003 Å
• b: 38.235 ± 0.004 Å
• c: 26.324 ± 0.003 Å
• α: 90°
• β: 99.404 ± 0.002°
• γ: 90°
• Cell volume: 27806 ± 5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0615
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.1377
• Weighted residual factors for all reflections included in the refinement: 0.1433
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No