Information card for entry 7125736

Structure parameters

• Chemical name: 3D-T4-SnOS
• Formula: C48 H133 N9 O23 S32 Sn20
• Calculated formula: O10 S32 Sn20
• Title of publication: A wide pH-range stable crystalline framework based on the largest tin-oxysulfide cluster [Sn₂₀O₁₀S₃₄].
• Authors of publication: Huang, Shan-Lin; He, Liang; Chen, Er-Xia; Lai, Heng-Dong; Zhang, Jian; Lin, Qipu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2019
• Journal volume: 55
• Journal issue: 74
• Pages of publication: 11083 - 11086
• a: 23.5105 ± 0.0004 Å
• b: 23.5105 ± 0.0004 Å
• c: 40.205 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 22223.1 ± 1.7 ų
• Cell temperature: 99.99 ± 0.16 K
• Ambient diffraction temperature: 99.99 ± 0.16 K
• Number of distinct elements: 6
• Space group number: 142
• Hermann-Mauguin space group symbol: I 41/a c d :2
• Hall space group symbol: -I 4bd 2c
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1077
• Weighted residual factors for all reflections included in the refinement: 0.1173
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No