Information card for entry 7125843

Structure parameters

• Formula: C42 H47 N
• Calculated formula: C42 H47 N
• Title of publication: Access to the most sterically crowded anilines via non-catalysed C-C coupling reactions.
• Authors of publication: Vrána, Jan; Samsonov, Maksim A.; Němec, Vlastimil; RůŽička, Aleš
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 16
• Pages of publication: 2487 - 2490
• a: 6.3152 ± 0.0002 Å
• b: 10.7638 ± 0.0003 Å
• c: 24.7246 ± 0.0008 Å
• α: 85.9667 ± 0.0013°
• β: 87.0612 ± 0.0015°
• γ: 88.1823 ± 0.0014°
• Cell volume: 1673.63 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No