Information card for entry 7125849

Structure parameters

• Formula: C27 H38 B Cl N6 Ni
• Calculated formula: C27 H38 B Cl N6 Ni
• Title of publication: Nickel(ii)-methyl complexes adopting unusual seesaw geometries.
• Authors of publication: Hill, Ethan A.; Zhao, Norman; Filatov, Alexander S.; Anderson, John S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 57
• Pages of publication: 7861 - 7864
• a: 9.6383 ± 0.0016 Å
• b: 17.821 ± 0.003 Å
• c: 16.177 ± 0.003 Å
• α: 90°
• β: 91.925 ± 0.006°
• γ: 90°
• Cell volume: 2777.1 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0633
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.0847
• Weighted residual factors for all reflections included in the refinement: 0.0939
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No