Information card for entry 7125963

Structure parameters

• Formula: C112 H184 K4 N8 O27
• Calculated formula: C112 H184 K4 N8 O27
• Title of publication: Stable, yet "naked", azo radical anion ArNNAr^- and dianion ArNNAr^2- (Ar = 4-CN-2,6-ⁱPr₂-C₆H₂) with selective CO₂ activation.
• Authors of publication: Wang, Wenqing; Tan, Gengwen; Feng, Rui; Fang, Yong; Chen, Chao; Ruan, Huapeng; Zhao, Yue; Wang, Xinping
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 22
• Pages of publication: 3285 - 3288
• a: 13.5116 ± 0.0006 Å
• b: 14.2386 ± 0.0008 Å
• c: 17.4578 ± 0.0008 Å
• α: 84.41 ± 0.002°
• β: 68.71 ± 0.001°
• γ: 86.045 ± 0.002°
• Cell volume: 3112.5 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0979
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.1917
• Weighted residual factors for all reflections included in the refinement: 0.2123
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No