Information card for entry 7126219

Structure parameters

• Formula: C47 H47 Al F36 N4 O4 Si
• Calculated formula: C47 H47 Al F36 N4 O4 Si
• Title of publication: N-H cleavage vs. Werner complex formation: reactivity of cationic group 14 tetrelenes towards amines.
• Authors of publication: Do, Dinh Cao Huan; Protchenko, Andrey V.; Fuentes, M Ángeles; Hicks, Jamie; Vasko, Petra; Aldridge, Simon
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 34
• Pages of publication: 4684 - 4687
• a: 13.993 ± 0.0001 Å
• b: 19.5525 ± 0.0002 Å
• c: 21.6682 ± 0.0002 Å
• α: 90°
• β: 98.012 ± 0.001°
• γ: 90°
• Cell volume: 5870.51 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0965
• Residual factor for significantly intense reflections: 0.0852
• Weighted residual factors for significantly intense reflections: 0.2387
• Weighted residual factors for all reflections included in the refinement: 0.2547
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No