Crystallography Open Database

Information card for entry 7126332

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Coordinates	7126332.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C85 H75 N4 Ni2 P4 Si2
Calculated formula	C85 H75 N4 Ni2 P4 Si2
Title of publication	Semi-bridging σ-silyls as Z-type ligands.
Authors of publication	Frogley, Benjamin J.; Hill, Anthony F.; Sharma, Manab; Sinha, Arup; Ward, Jas S.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	24
Pages of publication	3532 - 3535
a	12.6509 ± 0.0003 Å
b	16.9249 ± 0.0006 Å
c	17.6665 ± 0.0006 Å
α	81.189 ± 0.0012°
β	77.4286 ± 0.0016°
γ	73.2272 ± 0.0017°
Cell volume	3518.3 ± 0.2 Å³
Cell temperature	200 K
Ambient diffraction temperature	200 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.073
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.0942
Weighted residual factors for all reflections included in the refinement	0.1071
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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