Information card for entry 7126393
| Formula |
C63 H60 N2 O8 P2 |
| Calculated formula |
C63 H60 N2 O8 P2 |
| Title of publication |
A three-component reaction of phosphorus ylides with isocyanates: facile synthesis of 2-amino-3-carboxylate-4-quinolones. |
| Authors of publication |
Babu, Kaki Raveendra; Han, Wendan; Chen, Jian-Bo; Li, Yang; Tang, Yuhai; Zhang, Wenquan; Xu, Wenbo; Xu, Silong |
| Journal of publication |
Chemical communications (Cambridge, England) |
| Year of publication |
2020 |
| Journal volume |
56 |
| Journal issue |
44 |
| Pages of publication |
5909 - 5912 |
| a |
33.89 ± 0.02 Å |
| b |
9.68 ± 0.007 Å |
| c |
18.339 ± 0.013 Å |
| α |
90° |
| β |
115.521 ± 0.009° |
| γ |
90° |
| Cell volume |
5429 ± 6 Å3 |
| Cell temperature |
296 ± 2 K |
| Ambient diffraction temperature |
296 ± 2 K |
| Number of distinct elements |
5 |
| Space group number |
15 |
| Hermann-Mauguin space group symbol |
C 1 2/c 1 |
| Hall space group symbol |
-C 2yc |
| Residual factor for all reflections |
0.1032 |
| Residual factor for significantly intense reflections |
0.0658 |
| Weighted residual factors for significantly intense reflections |
0.1887 |
| Weighted residual factors for all reflections included in the refinement |
0.221 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.024 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/7126393.html
