Information card for entry 7126472

Structure parameters

• Formula: C16 H38 Cl2 Ni O2 P2
• Calculated formula: C16 H38 Cl2 Ni O2 P2
• Title of publication: Unexpected reactivity of a PONNOP 'expanded pincer' ligand.
• Authors of publication: Scheerder, Arthur R.; Lutz, Martin; Broere, Daniël L J
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 59
• Pages of publication: 8198 - 8201
• a: 7.8506 ± 0.0007 Å
• b: 8.205 ± 0.0005 Å
• c: 9.6512 ± 0.0008 Å
• α: 111.818 ± 0.004°
• β: 100.304 ± 0.003°
• γ: 97.698 ± 0.003°
• Cell volume: 554 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0801
• Residual factor for significantly intense reflections: 0.0536
• Weighted residual factors for significantly intense reflections: 0.1247
• Weighted residual factors for all reflections included in the refinement: 0.1351
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No