Information card for entry 7126582

Structure parameters

• Formula: C14 H22 B N O2
• Calculated formula: C14 H22 B N O2
• Title of publication: ortho-Dialkylamino arylboranes as efficient reagents for difluorocarbene trapping.
• Authors of publication: Ilin, Egor A.; Smirnov, Vladimir O.; Volodin, Alexander D.; Korlyukov, Alexander A.; Dilman, Alexander D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 52
• Pages of publication: 7140 - 7142
• a: 17.0129 ± 0.001 Å
• b: 12.3612 ± 0.0007 Å
• c: 27.5884 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5801.8 ± 0.6 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0892
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1364
• Weighted residual factors for all reflections included in the refinement: 0.164
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No