Information card for entry 7126642

Structure parameters

• Formula: C71 H60 Cl6 Fe2 P4 Rh2
• Calculated formula: C71 H60 Cl6 Fe2 P4 Rh2
• Title of publication: Halogenation of A-frame μ-carbido complexes: a diamagnetic rhodium(ii) carbido complex.
• Authors of publication: Barnett, Harrison J.; Hill, Anthony F.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 56
• Pages of publication: 7738 - 7740
• a: 13.1742 ± 0.0003 Å
• b: 26.8362 ± 0.0006 Å
• c: 18.2963 ± 0.0003 Å
• α: 90°
• β: 90.747 ± 0.002°
• γ: 90°
• Cell volume: 6468 ± 0.2 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.074
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No