Information card for entry 7126648

Structure parameters

• Formula: C29 H46 B2 F8 N4 Ni O9 P4
• Calculated formula: C29 H46 B2 F8 N4 Ni O9 P4
• Title of publication: Facile synthesis of a nickel(0) phosphine complex at ambient temperature.
• Authors of publication: Hanf, Schirin; Grell, Toni; Waters, Jessica E.; García-Rodríguez, Raúl; Hey-Hawkins, Evamarie; Wright, Dominic S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 57
• Pages of publication: 7893 - 7896
• a: 8.9718 ± 0.0003 Å
• b: 14.0281 ± 0.0004 Å
• c: 17.394 ± 0.0006 Å
• α: 81.344 ± 0.003°
• β: 82.327 ± 0.003°
• γ: 74.196 ± 0.003°
• Cell volume: 2072.54 ± 0.12 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0725
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1248
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No