Information card for entry 7126709

Structure parameters

• Formula: C25 H34 Cl N O Si2
• Calculated formula: C25 H34 Cl N O Si2
• Title of publication: Palladium-catalyzed intermolecular C-H silylation initiated by aminopalladation.
• Authors of publication: Ji, Xiaoming; Wei, Feng; Wan, Bin; Cheng, Cang; Zhang, Yanghui
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 56
• Pages of publication: 7801 - 7804
• a: 8.8523 ± 0.0015 Å
• b: 9.551 ± 0.002 Å
• c: 16.927 ± 0.004 Å
• α: 81.918 ± 0.004°
• β: 78.36 ± 0.004°
• γ: 64.955 ± 0.006°
• Cell volume: 1267.5 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0422
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1029
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No