Information card for entry 7126751

Structure parameters

• Formula: C34 H34 N4 Si2
• Calculated formula: C34 H34 N4 Si2
• Title of publication: Insertion of Ni(0) and Pd(0) precursors into the Si-Si bond of a disilane with two hypercoordinate silicon atoms.
• Authors of publication: Usui, Ryosuke; Sunada, Yusuke
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 60
• Pages of publication: 8464 - 8467
• a: 10.379 ± 0.003 Å
• b: 9.789 ± 0.002 Å
• c: 14.974 ± 0.004 Å
• α: 90°
• β: 105.172 ± 0.004°
• γ: 90°
• Cell volume: 1468.3 ± 0.7 ų
• Cell temperature: 203 K
• Ambient diffraction temperature: 203 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0632
• Residual factor for significantly intense reflections: 0.051
• Weighted residual factors for significantly intense reflections: 0.1245
• Weighted residual factors for all reflections included in the refinement: 0.1322
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No