Crystallography Open Database

Information card for entry 7126773

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Coordinates	7126773.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H28 Cl N2 O Rh
Calculated formula	C25 H28 Cl N2 O Rh
Title of publication	Rhodium(iii)-catalyzed diamidation of olefins via amidorhodation and further amidation.
Authors of publication	Wang, Jinlei; Zheng, Guangfan; Li, Xingwei
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	56
Pages of publication	7809 - 7812
a	11.9749 ± 0.0004 Å
b	15.7608 ± 0.0005 Å
c	23.8262 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	4496.8 ± 0.2 Å³
Cell temperature	153 K
Ambient diffraction temperature	153.02 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0241
Residual factor for significantly intense reflections	0.0237
Weighted residual factors for significantly intense reflections	0.0577
Weighted residual factors for all reflections included in the refinement	0.058
Goodness-of-fit parameter for all reflections included in the refinement	1.1
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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