Information card for entry 7126781

Structure parameters

• Formula: C24 H60 O18 V6
• Calculated formula: C24 H60 O18 V6
• Title of publication: Mechanistic insights into polyoxometalate self-assembly in organic solvent: conversion of a cyclic polyoxovanadate-ethoxide to its Lindqvist congener.
• Authors of publication: Meyer, Rachel L.; Love, Robert; Brennessel, William W.; Matson, Ellen M.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 61
• Pages of publication: 8607 - 8610
• a: 16.3679 ± 0.0001 Å
• b: 16.3679 ± 0.0001 Å
• c: 16.3679 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4385.09 ± 0.05 ų
• Cell temperature: 173 ± 0.1 K
• Ambient diffraction temperature: 173 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 205
• Hermann-Mauguin space group symbol: P a -3
• Hall space group symbol: -P 2ac 2ab 3
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0797
• Weighted residual factors for all reflections included in the refinement: 0.0807
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No