Information card for entry 7126813

Structure parameters

• Formula: C118 H214 N2 O28 Si16 Yb2
• Calculated formula: C118 H214 N2 O28 Si16 Yb2
• Title of publication: Structure and small molecule activation reactivity of a metallasilsesquioxane of divalent ytterbium.
• Authors of publication: Willauer, Aurélien R; Dabrowska, Anna M.; Scopelliti, Rosario; Mazzanti, Marinella
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 63
• Pages of publication: 8936 - 8939
• a: 16.342 ± 0.002 Å
• b: 23.291 ± 0.003 Å
• c: 24.187 ± 0.004 Å
• α: 113.031 ± 0.009°
• β: 90.664 ± 0.014°
• γ: 100.204 ± 0.01°
• Cell volume: 8305 ± 2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1028
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1533
• Weighted residual factors for all reflections included in the refinement: 0.1771
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No