Information card for entry 7126882

Structure parameters

• Formula: C67 H56 Br Cl3 F3 N O3 Os P4 S
• Calculated formula: C67 H56 Br Cl3 F3 N O3 Os P4 S
• Title of publication: Conventional and unconventional alkyne activations by Ru and Os for unprecedented dimetalated quinolizinium complexes.
• Authors of publication: Yeung, Chi-Fung; Chung, Lai-Hon; Tse, Sheung-Ying; Shek, Hau-Lam; Tse, Man-Kit; Yiu, Shek-Man; Wong, Chun-Yuen
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 63
• Pages of publication: 8908 - 8911
• a: 13.0222 ± 0.0004 Å
• b: 14.4045 ± 0.0005 Å
• c: 19.6691 ± 0.0006 Å
• α: 79.101 ± 0.001°
• β: 71.46 ± 0.001°
• γ: 85.621 ± 0.001°
• Cell volume: 3434.4 ± 0.19 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.0399
• Weighted residual factors for significantly intense reflections: 0.0982
• Weighted residual factors for all reflections included in the refinement: 0.1036
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No