Information card for entry 7126884

Structure parameters

• Formula: C69 H62 F6 N O7.5 Os P4 S2
• Calculated formula: C69 H62 F6 N O7.5 Os P4 S2
• Title of publication: Conventional and unconventional alkyne activations by Ru and Os for unprecedented dimetalated quinolizinium complexes.
• Authors of publication: Yeung, Chi-Fung; Chung, Lai-Hon; Tse, Sheung-Ying; Shek, Hau-Lam; Tse, Man-Kit; Yiu, Shek-Man; Wong, Chun-Yuen
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 63
• Pages of publication: 8908 - 8911
• a: 23.062 ± 0.0005 Å
• b: 16.4101 ± 0.0004 Å
• c: 36.9903 ± 0.0009 Å
• α: 90°
• β: 104.016 ± 0.001°
• γ: 90°
• Cell volume: 13582.2 ± 0.6 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0924
• Residual factor for significantly intense reflections: 0.0801
• Weighted residual factors for significantly intense reflections: 0.2347
• Weighted residual factors for all reflections included in the refinement: 0.2526
• Goodness-of-fit parameter for all reflections included in the refinement: 1.156
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No