Information card for entry 7126965

Structure parameters

• Formula: C22 H25 N O8
• Calculated formula: C22 H25 N O8
• Title of publication: Collective enantioselective total synthesis of (+)-sinensilactam A, (+)-lingzhilactone B and (-)-lingzhiol: divergent reactivity of styrene.
• Authors of publication: Zhang, Da-Wei; Fan, Hui-Lan; Zhang, Wenzhao; Li, Cheng-Ji; Luo, Sanzhong; Qin, Hong-Bo
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 69
• Pages of publication: 10066 - 10069
• a: 18.9306 ± 0.0014 Å
• b: 11.0428 ± 0.0008 Å
• c: 21.1989 ± 0.0016 Å
• α: 90°
• β: 114.695 ± 0.001°
• γ: 90°
• Cell volume: 4026.3 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0842
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1096
• Weighted residual factors for all reflections included in the refinement: 0.1259
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No