Information card for entry 7127189

Structure parameters

• Formula: C119.5 H108 Cl4 P8 Rh4 S2
• Calculated formula: C119.5 H108 Cl4 P8 Rh4 S2
• Title of publication: Dimetalla-heterocyclic carbenes: the interconversion of chalcocarbonyl and carbido ligands.
• Authors of publication: Barnett, Harrison J.; Hill, Anthony F.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 83
• Pages of publication: 12593 - 12596
• a: 16.3139 ± 0.0003 Å
• b: 19.5375 ± 0.0003 Å
• c: 22.4893 ± 0.0004 Å
• α: 71.332 ± 0.002°
• β: 72.996 ± 0.002°
• γ: 79.948 ± 0.002°
• Cell volume: 6468.1 ± 0.2 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0858
• Residual factor for significantly intense reflections: 0.0728
• Weighted residual factors for significantly intense reflections: 0.2055
• Weighted residual factors for all reflections included in the refinement: 0.2249
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No