Information card for entry 7127266

Structure parameters

• Formula: C34 H64 N4 Si4 Yb
• Calculated formula: C34 H64 N4 Si4 Yb
• Title of publication: Ln(II) amido complexes coordinated by ring-expanded N-heterocyclic carbenes - promising catalysts for olefin hydrophosphination.
• Authors of publication: Lapshin, Ivan V.; Cherkasov, Anton V.; Asachenko, Andrey F.; Trifonov, Alexander A.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 85
• Pages of publication: 12913 - 12916
• a: 15.5992 ± 0.0007 Å
• b: 11.4432 ± 0.0005 Å
• c: 23.1873 ± 0.0009 Å
• α: 90°
• β: 94.693 ± 0.002°
• γ: 90°
• Cell volume: 4125.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0336
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.0678
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No