Information card for entry 7127290

Structure parameters

• Formula: C25 H21 F9 N4 O9.5 S3 Sb
• Calculated formula: C25 H21 F9 N4 O9.5 S3 Sb
• Title of publication: An arene-stabilized η⁵-pentamethylcyclopentadienyl antimony dication acts as a source of Sb⁺ or Sb³⁺ cations.
• Authors of publication: Zhou, Jiliang; Kim, Hyehwang; Liu, Liu Leo; Cao, Levy L.; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 85
• Pages of publication: 12953 - 12956
• a: 9.101 ± 0.0004 Å
• b: 13.275 ± 0.0006 Å
• c: 13.8328 ± 0.0006 Å
• α: 81.615 ± 0.002°
• β: 86.39 ± 0.002°
• γ: 84.352 ± 0.002°
• Cell volume: 1643.32 ± 0.13 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0364
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.0929
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No