Information card for entry 7128003

Structure parameters

• Formula: C64 H58 B F24 O Sb
• Calculated formula: C64 H58 B F24 O Sb
• Title of publication: Unsupported monomeric stibine oxides (R₃SbO) remain undiscovered.
• Authors of publication: Wenger, John S.; Johnstone, Timothy C.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 28
• Pages of publication: 3484 - 3487
• a: 12.7443 ± 0.0004 Å
• b: 13.0965 ± 0.0004 Å
• c: 20.1296 ± 0.0007 Å
• α: 76.697 ± 0.003°
• β: 79.142 ± 0.003°
• γ: 78.266 ± 0.003°
• Cell volume: 3165.73 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.06
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for significantly intense reflections: 0.1342
• Weighted residual factors for all reflections included in the refinement: 0.1399
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No