Information card for entry 7128196

Structure parameters

• Formula: C72 H60 F Ge P3 Pd
• Calculated formula: C72 H60 F Ge P3 Pd
• SMILES: [Pd]12([Ge](F)(c3ccccc3)(c3ccccc3[P]2(c2ccccc2)c2ccccc2)c2ccccc2[P]1(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1.c1ccccc1.c1ccccc1
• Title of publication: Pd/Ni-Catalyzed Germa-Suzuki coupling <i>via</i> dual Ge-F bond activation.
• Authors of publication: Kameo, Hajime; Mushiake, Akihiro; Isasa, Tomohito; Matsuzaka, Hiroyuki; Bourissou, Didier
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 41
• Pages of publication: 5004 - 5007
• a: 13.3586 ± 0.0012 Å
• b: 14.0431 ± 0.0016 Å
• c: 16.711 ± 0.002 Å
• α: 109.543 ± 0.005°
• β: 96.454 ± 0.002°
• γ: 98.884 ± 0.003°
• Cell volume: 2873.2 ± 0.6 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0614
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.0955
• Weighted residual factors for all reflections included in the refinement: 0.1033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.710747 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No