Information card for entry 7128571

Structure parameters

• Formula: C23 H33 N O2 Si
• Calculated formula: C23 H33 N O2 Si
• Title of publication: Direct formation of 4,5-disubstituted carbazoles via regioselective dilithiation.
• Authors of publication: Pocock, Ian A.; Alotaibi, Alya M.; Jagdev, Kesar; Prior, Connor; Burgess, Gregory R.; Male, Louise; Grainger, Richard S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 59
• Pages of publication: 7252 - 7255
• a: 19.2612 ± 0.0006 Å
• b: 19.2612 ± 0.0006 Å
• c: 9.9892 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3209.4 ± 0.2 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 169
• Hermann-Mauguin space group symbol: P 61
• Hall space group symbol: P 61
• Residual factor for all reflections: 0.0684
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1663
• Weighted residual factors for all reflections included in the refinement: 0.1764
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No