Information card for entry 7128638

Structure parameters

• Formula: C33 H74 Cl2 Mo9 N2 O41 P V4
• Calculated formula: C33 H74 Cl2 Mo9 N2 O41 P V4
• Title of publication: Synthesis of a phosphomolybdate with a tetranuclear vanadium core by installing vanadium atoms in a lacunary template using the protecting group strategy.
• Authors of publication: Li, Chifeng; Yamaguchi, Kazuya; Suzuki, Kosuke
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 64
• Pages of publication: 7882 - 7885
• a: 55.5617 ± 0.0014 Å
• b: 14.4627 ± 0.0002 Å
• c: 24.0687 ± 0.0006 Å
• α: 90°
• β: 117.802 ± 0.003°
• γ: 90°
• Cell volume: 17108.3 ± 0.8 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1177
• Residual factor for significantly intense reflections: 0.0777
• Weighted residual factors for significantly intense reflections: 0.1682
• Weighted residual factors for all reflections included in the refinement: 0.1867
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No